INVESTIGATION ON THE STRUCTURAL, MAGNETIC, AND DIELECTRIC PROPERTIES OF MG2+ SUBSTITUTED NI-CD-IN SPINEL NANOSTRUCTURED FERRITES SYNTHESIZED BY COPRECIPITATION ROUTE
DOI:
https://doi.org/10.29121/shodhkosh.v5.i2.2024.5055Keywords:
Xrd, Ftir, Vsm and Dielectric SpectroscopyAbstract [English]
A soft spinel ferrite has the chemical formula MgxNi0.6Cd0.4-xFe2-yInyO4, where X values are 0.0, 0.1, 0.2, 0.3, and 0.4, and y is fixed at 0.05. These are labelled as GK6, GK7, GK8, GK9, and GK10 and are made using the coprecipitation method. X-ray diffraction patterns show that the crystallite size decreases from 21 nm to 10 nm, and the lattice dimension shrinks from 8.4839 to 8.4175 Å. FTIR analysis shows a strong vibrational band for the Fe-O group between 400 and 4000 cm⁻¹, which confirms the formation of spinel ferrite. VSM analysis indicates that coercivity increases from 297 to 338 Oe. However, retentivity decreases from 8.87 to 1.99 emu/g, and magnetic saturation drops from 54 to 22 emu/g. The impedance analyzer shows lower losses at high frequencies, suggesting that this material is suitable for microwave devices.
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Copyright (c) 2024 Dilip S. Badwaik, Gaurav Kale, Dnyaneshwar D. Mathankar, Sarang R. Daf, Shrikant M. Suryawanshi

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